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Beilstein J. Org. Chem. 2012, 8, 1344–1351, doi:10.3762/bjoc.8.154
Graphical Abstract
Scheme 1: Retrosynthetic strategy.
Scheme 2: Macrolactonization reactions of seco acids 5 and 6 (for reagents and yields see Table 1 and Table 2).
Figure 1: Analytical HPLC traces of linear peptides. (a) Compound 9 (retention time = 31.5 min); (b) Compound ...
Scheme 3: Synthesis of the dehydroxy side chain 12.
Scheme 4: Synthesis of LI-F04a (1) and analogues 20–23.
Figure 2: Structures and lowest-energy conformers of 24 (left) and 25 (right) obtained using Macromodel. Hydr...